Triazole fungicide has demonstrated a great potential in wood preservation. In order to develop a short synthetic route of triazole fungicides—1-（ 1H-1,2,4-triazole-1-yl）-2-tert-butyl-3 （ 4-chlorophenoxy） 2-propanol,the authors investigated the effects of molar ratio,reaction temperature,and reaction time on the yield of the target compound and evaluated its bacteriostasis. The result showed that the yield of the target compound was about 62% ,under the mole ratio of 1-（2-tert-butyl-2,3-epoxy propyl） 1h-1,4 trichlorobenzene triazole methane sulfonate to p-chlorophenol to sodium hydride 1∶ 1. 2∶ 1. 38,temperature 60 ℃ for 6 h. The target compound also showed promising inhibitory effect on the selected mold and woodrotting fungi.